Adhesives & Adhesive Tapes Testing Guide

Adhesives are one of the most widely tested products because of this there are 100’s of different tests and test methods. This is also the same for adhesive tapes testing.  Adhesives are critical to just about every part of our lives and are used in so many industries and products. As such, understanding the adhesive qualities and limiting factors are integral to a wide range of industries. The main type of test is a peel test and these can be broken down into 6 main versions of peel strength tests. Each of these adhesives or tapes will have been tested in both the development stage and as part of the manufacturing process to ensure consistent quality.  This guide will discuss each of these peel types of tests and how it’s critical to perform the correct peel test for your material and or application. As you can see from this short guide there are many types and subtypes of peel test.  AML are on hand to help determine the correct test & method for your needs, do not hesitate to contact us for friendly and professional advice or for a quotation for the test equipment required for your particular test or how to perform the test.  After selection of the correct type of peel test, the next most important part of the test is the sample preparation, each of the standards listed in this guide will have an exact method of sample preparation. We are on hand to help with this too.  Before attempting any adhesive tests you should study the relevant standard to ensure the test is performed exactly as stated, any deviation from the published method will mean significant errors in the data collected from the test. 

180 Degree Peel Tests

A tensile tester and grips or special fixture are used along with a test panel, to apply a force at 180 degrees to the panel. The 180-degree peel test is best suited to a flexible material that is bonded to a rigid substrate.  180 Degree Peel Test The image below shows a special fixture for holding the test panel, this type of fixture makes the test easier to complete and more reproducible. Holder for Testing Panel The test panels are generally float glass or stainless steel. The specifications of the test panels, test speed and method of specimen preparation are specified in the relevant standard and test method followed.  180-degree peel tests are also widely performed in heat-sealed applications such as packaging; this differs as it doesn’t use a test panel and is generally called a T peel test, see later in this guide for a description of this T peel method. 

180 Degree Peel Test Methods and Standards

ASTM 180 Degree Peel Test Methods

ASTM-D3330 - A – Standard Test Method for Peel Adhesion of Pressure-Sensitive Tape ASTM-F88 – Standard Test Method for Seal Strength of Flexible Barrier Materials ASTM-D3330 - B - E – Standard Test Method for Peel Adhesion of Pressure-Sensitive Tape ASTM-D903 – Standard Test Method for Peel or Stripping Strength of Adhesive Bonds ASTM-D5458 – Standard Test Method for Peel Cling of Stretch Wrap Film

ISO Peel Test Methods

ISO-8510-2 – Adhesives - Peel test for a flexible-bonded-to-rigid test specimen assembly - Part 2: 180-degree peel ISO-11607-1 – Packaging for terminally sterilized medical devices - Part 1: Requirements for materials, sterile barrier systems and packaging systems

BS 180 Degree Peel Test

BS EN-1939 – Self-adhesive tapes. Determination of peel adhesion properties BS EN ISO-8510-2 – Adhesives. Peel test for a flexible-bonded-to-rigid test specimen assembly. 180-degree peel

Finat 180 Degree Peel Test

FINAT is the European association for the self-adhesive label industry. It also covers adjacent narrow-web product decoration and identification technologies. FINAT-FTM1 – Peel adhesion (180°) at 300 mm per minute FINAT-FTM3 – Low-speed release force

Afera 180 Degree Peel Test

Afera is the European Adhesive Tape Association, is the European trade association for adhesive tapes. Afera-5001 – Self Adhesive Tapes - Measurement of Peel Adhesion from Stainless Steel or from its own Backing

PSTC 180 Degree Peel Tests 

The Pressure Sensitive Tape Council (PSTC) is the North American trade association for the pressure-sensitive tape industry.   PSTC-101 – International Standard for Peel Adhesion of Pressure Sensitive Tape PSTC-4 – Relative performance of release coatings PSTC-8 – unwind force of pressure-sensitive tape

TLMI 180 Degree Peel Tests

TLMI is a trade association for the adhesive labels industry.  TLMI-L-IA1 – 180° peel adhesion - face stock TLMI-L-IA2 – 180° peel adhesion - release liner

SAE 180 Degree Peel Methods

SAE-J 1907 – Peel Adhesion Test for Glass to Elastomeric Material for automotive glass Encapsulation

90 Degree Peel Tests

A tensile tester, grips and special fixture are used along with a test panel or part under test, applying a force at 90 degrees to the panel or part being tested. The 90-degree peel test is suitable for a flexible material that is bonded to a rigid substrate.  90 Degree Peel Tests In the image below you can see a 90-degree peel table.  90 Degree Peel Test Example Depending on the shape or size of the specimen or test panel these peel tables can be configured in many different ways. For information on the correct configuration and details on the test panel, the relevant standard or test method should be consulted, or contact AML for help and advice. In a similar manner to the 180-degree test panels, these are often float glass or stainless steel, the properties, method or specimen preparation are closely controlled to ensure repeatability and reproducibility. 

ASTM 90 Degree Peel Tests

ASTM-D6252 – Standard Test Method for Peel Adhesion of Pressure-Sensitive Label Stocks at a 90° Angle ASTM-D3330 – Standard Test Method for Peel Adhesion of Pressure-Sensitive Tape ASTM-B533 – Standard Test Method for Peel Strength of Metal Electroplated Plastics ASTM-B571-97 – Standard Practice for Qualitative Adhesion Testing of Metallic Coatings ASTM-D816 – Standard Test Methods for Rubber Cements ASTM-D429 – Standard Test Methods for Rubber Property—Adhesion to Rigid Substrates ASTM-D6862 – Standard Test Method for 90 Degree Peel Resistance of Adhesives

BS 90 Degree Peel Tests

BS EN-1939 – Self-adhesive tapes. Determination of peel adhesion properties BS EN-2243-3 – Aerospace series. Non-metallic materials. Structural adhesives. Test method. Peeling test metal-honeycomb core BS EN-28510-1 – Adhesives. Peel test for a flexible-bonded-to-rigid test specimen assembly. 90° peel

ISO  90 Degree Peel Tests

ISO-8510-1 – Adhesives - Peel test for a flexible-bonded-to-rigid test specimen assembly - Part 1: 90-degree peel

SAE  90 Degree Peel Tests

SAE-J 1553 – Cross Peel Test for Automotive-Type Adhesives for Fiber reinforced plastic (FRP) Bonding

FINAT 90 Degree Peel Tests

FINAT-FTM2 – Peel adhesion (90°) at 300 mm per minute

IPC 90 Degree Peel Tests

IPC-TM-650 – IPC-TM-650 Test Methods Manual

AFERA 90 Degree Peel Tests

Afera-5001 – Self Adhesive Tapes - Measurement of Peel Adhesion from Stainless Steel or from its own Backing

Climbing Drum Peel Test

The climbing drum peel test often referred to as the German wheel peel test is a less common test but can also be used where a flexible material and rigid substrate requires testing.  Climbing Drum Peel Test Diagram In the image below there is a German Peel Wheel. Peel wheel tests are easy to perform and less fiddly to set up compared to a 90-degree peel table test.  German Peel Wheel The image below shows the type of climbing drum peel test used on composites honeycomb panels typically to the requirements of  ASTM D1781, EN 2243-3 or DIN 53295. Climbing Drum Peel Test

DIN Climbing Drum Peel Tests

DIN 53357-B

ISO Climbing Drum Peel Tests

ISO 6133

ATSM Climbing Drum Peel Tests

ASTM-D1781 – Standard Test Method for Climbing Drum Peel for Adhesives ASTM-D1995 – Standard Test Methods for Multi-Modal Strength Testing of Adhesives 

Floating Roller Peel Tests

Floating Roller Peel Tests The Floating Roller Peel Test. There are many types of peel fixtures for this type of peel test. The floating roller test is similar to the other tests described so far in this article are for a rigid or semi-rigid substrate and flexible material. The rollers are generally set at 90 or 115 degrees but we have options for adjustable angle fixtures. These rollers are set a small distance apart to allow the thin and flexible material to pass through them, this is attached to another grip attached to the tensile tester. This maintains the required test angle.    [gallery link="file" columns="2" size="medium" ids="96241,96242"]

ASTM Floating Roller Peel Tests

ASTM-D3167 – Standard Test Method for Floating Roller Peel Resistance of Adhesives

BS Floating Roller Peel Tests

BS EN-1372 – Adhesives. Test method for adhesives for floor and wall coverings. Peel test BS EN-1464 – Adhesives. Determination of peel resistance of high-strength adhesive bonds. Floating roller method BS EN-2243-2 – Aerospace series. Non-metallic materials. Structural adhesives. Test method. Peel metal-metal

DIN Floating Roller Peel Tests

DIN EN-1464 – Testing of adhesives for metals and adhesively bonded metal joints; floating roller peel test

ISO Floating Roller Peel Tests

ISO-10373-1 – Identification cards - Test methods - Part 1: General characteristics ISO-14676 – Adhesives - Evaluation of the effectiveness of surface treatment techniques for aluminium - Wet-peel test by the floating-roller method ISO-4578 – Adhesives - Determination of peel resistance of high-strength adhesive bonds - Floating-roller method

Loop Tack Adhesive & Tape Testing

Loop tack is the measure of the “initial grab” or “tack” of pressure-sensitive tapes or adhesives. Loop Tack Adhesive Testing A loop of material is brought into contact with the standard material, usually glass or stainless steel. The size of the loop and standard material size and specification along with the speed of the test are set down in the relevant standard. The test measures the force required to pull the tape or adhesive away from the test panel. 

Typical Standards for Loop Tack

FINAT-FTM 9 – Loop tack measurement ASTM-D6195 – Standard Test Methods for Loop Tack BS EN-1719 – Adhesives for paper and board, packaging and disposable sanitary products. Tack measurement for pressure-sensitive adhesives. Determination of loop tack PSTC-16 – Loop tack

T-Peel Tests

T Peel tests are usually performed when both the adhesive or tape has similar flexibility to the substrate. Both substrate & adhesive must be flexible to allow bending through 90 degrees without breaking. In the T peel test, the tails are unsupported so that the entire load is applied to the bond. T Peel Testing Diagram Of all the peel test methods this one tends to provide the lowest force values. When testing very low peel force materials the weight of the tails will affect the results obtained. This can also add significant variation to the results.  If testing an adhesive or tape to a more rigid substrate then the 90 or 180-degree methods are more suitable. 

ASTM T Peel Methods

ASTM-D1876 – Standard Test Method for Peel Resistance of Adhesives (T-Peel Test) ASTM-D1995 – Standard Test Methods for Multi-Modal Strength Testing of Adhesives (Contact Adhesives) ASTM-D2918 – Standard Test Method for Durability Assessment of Adhesive Joints Stressed in Peel ASTM-D413 – Standard Test Methods for Rubber Property—Adhesion to Flexible Substrate ASTM-D5170 – Standard Test Method for Peel Strength ('T' Method) of Hook and Loop Touch Fasteners ASTM-D6496 – Standard Test Method for Determining Average Bonding Peel Strength Between the Top and Bottom Layers of Needle-Punched Geosynthetic Clay Liners ASTM-F2256 – Standard Test Method for Strength Properties of Tissue Adhesives in T-Peel by Tension Loading ASTM-F88 – Standard Test Method for Seal Strength of Flexible Barrier Materials

BS T Peel Methods

BS EN-12242 – Touch and close fasteners. Determination of peel strength BS EN-1895 – Adhesives for paper and board, packaging and disposable sanitary products - 180°-'T' peel test for a flexible-to-flexible assembly BS EN-868-5 – Packaging materials and systems for medical devices which are to be sterilized. Heat and self-sealable pouches and reels of paper and plastic film construction. Requirements and test methods

ISO T-Test Methods 

ISO-11339 – Adhesives - T-peel test for flexible-to-flexible bonded assemblies ISO-20344 – Personal protective equipment - Test methods for footwear

Confused and not sure which method you need?

Contact us today for professional and friendly advice.  AML Instruments are leaders in the field of instrumentation and calibration. We pride ourselves on our competitive prices, reliable customer service and UKAS accreditation. AML is dedicated to providing the best solution and advice for your particular application, We do not source solutions from a single manufacturer so can offer you the very best equipment to match your requirements exactly. As well as standard solutions we can design and manufacture bespoke test equipment. Contact us today with your adhesive and tape testing challenge.

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